REFURBISHED INSTRUMENTS
Specifications

Type

Specification

GLP features

Early maintenance feedback (EMF), electronic records of
maintenance and errors

Communications

Controller-area network (CAN). GPIB (IEEE-448), RS232C,
APG-remote standard, optional four external contact closures and BCD vial number output

Safety features

Leak detection and safe leak handling, low voltages in maintenance areas, error detection and display

Injection range

0.1 – 100 μl in 0.1 μl increments
Up to 1500 μl with multiple draw (hardware modification required)

Replicate injections

1 – 99 from one vial

Precision

Typically < 0.5 % RSD of peak areas from 5 – 100 μl,
Typically < 1 % RSD of peak areas from 1 – 5 μl

Minimum sample volume

1 μl from 5 μl sample in 100 μl microvial, or 1 μl from 10 μl sample in 300 μl microvial

Carryover

Typically < 0.1 %, < 0.05 % with external needle cleaning

Sample viscosity     

range 0.2 – 50 cp

Replicate injections per vial

1 – 99

Sample capacity

100 × 2-ml vials in 1 tray
40 × 2-ml vials in ½ tray
15 × 6-ml vials in ½ tray (Agilent vials only)

Injection cycle time

Typically 50 s depending on draw speed and injection volume

Type

Specification

Hydraulic system

Dual plunger in series pump with proprietary servo-controlled variable stroke drive, floating plungers and active inlet valve

Setable flow range

0.001 – 10 ml/min, in 0.001 ml/min increments

Flow range

0.2 – 10.0 ml/min

Flow precision

< 0.3 % RSD (typically 0.15 %), based on retention time, at 1 ml/min

Pressure

Operating range 0 – 40 MPa (0 – 400 bar, 0 – 5880 psi) up to 5 ml/min Operating range 0 – 20 MPa (0 – 200 bar, 0 – 2950 psi) up to 10 ml/min

Pressure pulsation

< 2 %amplitude (typically < 1 %), at 1 ml/min isopropanol,
at all pressures > 1 MPa (10bar)

Compressibility compensation

User-selectable, based on mobile phase compressibility

Recommended pH

1.0 – 12.5, solvents with pH > 2.3 should not contain acids which attack

Range

stainless steel

Gradient formation

Low pressure quaternary mixing/gradient capability using proprietary
high-speed proportioning valve
Delay volume 800 – 1100 μl, dependent on back pressure

Composition Range

0 – 95 % or 5 – 100 %, user selectable

Composition Precision

< 0.2 % RSD, at 0.2 and 1 ml/min

Control and data evaluation

Agilent ChemStation for LC

Analog output

For pressure monitoring, 2 mV/bar, one output

Communications

Controller-area network (CAN), GPIB, RS-232C, APG Remote: ready, start, stop and shut-down signals, LAN optional

Type

Specification

Temperature range

10 degrees below ambient to 80 °C

Temperature stability

± 0.15 °C

Temperature accuracy

± 0.8 °C
± 0.5 °C With calibration

Column capacity

Three 30 cm

Warm-up/cool-down

5 minutes from ambient to 40 °C

Time

10 minutes from 40 – 20 °C

Dead volume

3 μl left heat exchanger

Dimensions

6 μl right heat exchanger
140 × 410 × 435 mm

(h × w × d)

(5.5 × 16 × 17 inches)

Weight   

10.2 kg (22.5 lbs)

Communications

Controller-area network (CAN), GPIB,
RS-232C, APG Remote: ready, start, stop
and shut-down signals, LAN optional

Type

Specification

Detection type

Double-beam photometer

Light source

Deuterium lamp

Wavelength range

190–600 nm

Short term noise

± 0.75 × 10-5 AU at 254 nm

(ASTM)

Drift

3 × 10-4 AU/hr at 254

Linearity

> 2 AU (5%) upper limit

Wavelength accuracy

± 1 nm Self-calibration with deuterium lines,

 

verification with holmium oxide filter

Band width

6.5 nm typical

Flow cells

Standard: 14-μl volume, 10-mm

 

cell path length and 40 bar

 

(588 psi) pressure maximum

 

High pressure: 14-μl volume,

 

10-mm cell path length and

 

400 bar (5880 psi) pressure

 

maximum

 

Micro: 1-μl volume, 5-mm cell

 

path length and 40 bar (588 psi)

 

pressure maximum

 

Semimicro: 5-μl volume, 6-mm

 

cell path length and 40 bar

 

(588 psi) pressure maximum

Control and data

Agilent ChemStation for LC

evaluation

Analog outputs

Recorder/integrator: 100 mV or

 

1 V, output range 0.001 – 2 AU,

 

one output

Communications

Controller-area network (CAN),

 

GPIB, RS-232C, APG Remote:

 

ready, start, stop and

 

shut-down signals, LAN

 

optional

Type

Specification

Detection type

1024-element photodiode array

Light source

Deuterium and tungsten lamps

Wavelength range

190 – 950 nm

Short term noise (ASTM)

± 1 × 10-5 AU at 254 and 750 nm

 

Single and Multi-Wavelength Drift

2 × 10-3 AU/hr at 254 nm

 

 

Linear absorbance range

> 2 AU (upper limit)

 

Wavelength accuracy

± 1 nm Self-calibration with deuterium lines,

 

verification with holmium oxide filter

Wavelength bunching

1 – 400 nm Programmable in steps of 1 nm

Slit width

1, 2, 4 , 8, 16 nm Programmable slit

Diode width

< 1 nm

Flow cells

Standard: 13 μl volume, 10 mm cell path

 

length and 120 bar (1760 psi)

 

pressure maximum

 

Semi-Micro: 5 μl volume, 6 mm cell

 

path length and 120 bar (1760 psi)

 

pressure maximum

 

High pressure: 1.7 μl volume, 6 mm cell

 

path length and 400 bar (5880 psi)

 

pressure maximum

 

500 nano: 0.5 μl volume, 10 mm cell

 

path length and 50 bar (725 psi)

 

pressure maximum

Control and data evaluation

Agilent ChemStation for LC

Analog outputs

Recorder/integrator: 100 mV or 1 V,

 

output range 0.001 – 2 AU, two outputs

Communications

Controller-area network (CAN), GPIB,

 

RS-232C, APG Remote: ready, start,

 

stop and shut-down signals, LAN optional

• Flow rates from 50 uL/min to 5 mL/min can be generated for use with 2.1 mm ID columns and larger.
• The autosampler has a maximum capacity of 120 vials (12×32, 2-mL) with programmable temperature control from 4 to 40°C.
• A heated column compartment provides temperatures from 5 degrees above ambient to 65°C.
• The detector is a photodiode array (model 2996) with a wavelength range of 190-800 nm and sensitivity settings from 0.0001-2.0000 absorbance units.

• Flow rates from 50 uL/min to 5 mL/min can be generated for use with 2.1 mm ID columns and larger.
• The autosampler has a maximum capacity of 120 vials (12×32, 2-mL) with programmable temperature control from 4 to 40°C.
• A heated column compartment provides temperatures from 5 degrees above ambient to 65°C.
• The detector is a photodiode array (model 2996) with a wavelength range of 190-800 nm and sensitivity settings from 0.0001-2.0000 absorbance units.

Refurbished TSP HPLC System comes with a TSP AS3000 Variable Volume Autosampler , TSP P1000 Isocratic Pump, and TSP UV 1000 Detector

The TSP AS3000 Autosampler provides outstanding
performance and maximum flexibility in an LC sample processing system. The
standard unit offers 120-vial capacity, multiple injection modes, random vial
access, re-use of calibration standards, and priority sampling

• Vial capacity:
– 120 vials in three removable trays
– 105 vials with tray temperature control

• Variable-Volume:
– Injection Precision: <0.5 % RSD @ 10 pL or greater
– Injection Volume: 0.1 – 100 pL injection standard (250 uL syringe) up to 1000 uL injections with larger loops and syringes

• Fixed-Loop:
– Injection Precision: <0.5% RSD @ 10 uL or greater
– Injection Volume: 20 uL standard (250 uL syringe) 1000 uL injections with larger loops and syringes

• Sample Carryover:
– <0.0 I% at 300 gL flush volume
– 5 mL flush volumes can be set

• Minimum Sample Volume: 1 uL can be injected from 5 uL with an end-port needle

• Needle Height: Programmable in 0.1 mm increments

• Method Files: Protected in non-volatile memory

• Communications
– Remote Inputs: Pump Ready, Inject Hold
– Outputs Pump Stop, Autosampler Ready, Inject, Gradient Start, Four timed-event outputs
– SpectraNETIRS-232 port

• Ambient Environment: 10° – 40°C, 5 – 95% relative humidity

• Dimensions: 37cm x 41 cmx 51 cm (HxWxD)

TSP UV 1000 Detector is a programmable variable single wavelength
detector. It has superior optical performance and has externally mounted
interchangeable flow cells for wide range of applications ranging from
capillary, microbore to preparative, CE, SFC and LC/MS.   

Wavelength Ranges: D2 lamp: 190 to 380 nm, W lamp: 366 to 800 nm

• Wavelength Accuracy: ± 1.0 nm
• Wavelength Precision: <0.01 nm

• Bandwidth: 6 nm
• Range Selections: 3.0, 2.0, 1.0, 0.5, 0.2, 0.1, 0.05, 0.02, 0.01, 0.005, 0.002, 0.001, 0.0005 AUFS
• Absorbance Range: 0.0005 to 3.0 AUFS
• Absorance Linearity @ 254 nm: 3.0 AUFS

Communications:
– Remote Inputs: Run, Stop, and Zero
– Remote Output: Ready

L-2130 HTA Pump Specifications
Accuracy
+/- 2 µL (0.01 to 0.10 mL/min)
+/- 2 % (0.101 to 8.000 mL/min)
+/- 4 % (8.001 to 9.999 mL/min)
Precision
+/-0.075 % RSD or 0.02 min SD at 1.0 mL/min
Constant pressure
290 to 5600 psi at 0 to 5.0 mL/min
Solvent delivery
100 µL stroke
Dimensions
13.5 in (W) x 15.75 in (D) x 6.0 in (D)
(340 mm (W) x 400 mm (D) x 150 mm (D))
Weight approx.
24 lbs (11 kg)
HIGH PRESSURE GRADIENT
Flow rate range
0.001 to 9.999 mL/min
(0.2 to 5.0 mL/min recommended)
Binary
Up to2 eluents
Composition range
1 to 100% (0.1% increments)
Accuracy
+/- 1 % (0.2 mL/min)
Precision
0.1% RSD or 0.02 min SD at 1.0 mL/min
LOW PRESSURE GRADIENT
Flow rate range
0.001 to 9.999 mL/min
(0.2 to 5.0 mL recommended)
Quarternary
Up to 4 eluents
Composition range
0 to 100% (0.1% increments with CDS; 1% increments with front panel control
Accuracy
+/- 1 % (0.2 mL/min)
Precision
0.1 % RSD or 0.02 min SD at 1.0 mL/min
L-2200 Autosampler SpecificationsL
Carry over
0.01% (< 0.003% with typical results)
Injection method
Direct all injection
Capacity
200 vials (1.5 mL)
Cooling options
4 to20 °C (at ambient)
Rack options
128 (4 mL), 336 (1 mL), Microtiter rack (3 plates)
Injection volume
0.1 to 50 µL (standard), 50 µL to 4.5 mL (optional)
Repeatability
0.3% RSD (at 10-µL injections)
% RSD of slopes
Correlation coefficient > 0.999
Response factor < 5% RSD
Max. # injections/vial
99
Max. cycle time
999.99
Min. cycle time
30 s
Syringe volumes
0.100 mL (standard), 0.5, 1, 2.5, and 5 mL (optional)
Safety
Built-in leak sensor
Dimensions
13.5 in (W) x 15.75 in (D) x 12.0 in (D)
(340 mm (W) x 400 mm (D) x300 mm (D))
Weight approx.
42 lbs (19 kg)
L-2300 Column Oven Specifications
Range
[Room temp - 15 °C] to[Room temp + 50°C] )
Setting range
1 to 65 °C
Accuracy
+/- 1 °C
Safety
Built-in vapor/leak sensor
Stability
+/- 0.1 °C
Column capacity
Up to three 25-cm columns
GLP functions
Serial number registration in unit memory
Dimensions
13.5 in (W) x 15.75 in (D) x 6.0 in (D)
(340 mm (W) x 400 mm (D) x 150mm (D))
Weight approx.
22 lbs (10 kg)
L-2490 RI Detector Specifications
Method of Detection
Deflection
Light source
Tungsten lamp
Refractive index range
1.0 to 1.75
Linearity range
600µRIU
Baseline noise
2.5 x 10-9 RIU or less (water filled in, time constant 3.0 s)
Temperature control
Off, 30 °C to 50 °C
Time constants
0.1, 0.25, 0.5, 1, 1.5, 2, 3, 6 s
External outputs
Warning when measurement range is exceeded, Auto zero, Alarm, Recorder 10 mV/FS, Integrator 1 V/FS
External inputs
Auto zero, Marker, Purge
Baseline adjustment range
0 to 50% /FS
Auto zero
Full auto zero (optics + calculation)
Recorder range
0.25 to 512 x 10-6 RIU/FS
Cell volume
8 µL
Max. flow rate
10 mL/min
Max. pressure in cell
7.1 psi (0.049 MPa)
Dimensions
13.5 in (W) x 15.75 in (D) x 6.0 in (D)
(340 mm (W) x 400 mm (D) x 150 mm (D))
Weight Approx.
29 lbs (13kg)
Power requirement & consumption
100 to 240 VAC (+/- 10%), 50/60 Hz, 150 VA or less
L-2485 Fluorescence Detector Specifications
Optics

Ratio-beam photometric detector using transmission light
Light source
150-W Xe lamp
Hg lamp for wavelength check
EX wavelength range and bandwidth
200 to 850 nm
15 nm
EM wavelength range and bandwidth
250 to 900 nm (over 731 nm requires PMT exchange)
15 nm and 30 nm
Sensitivity
S/N: >900 for Raman spectrum of water
(EX: 350 nm; time constant: 2 sec; bandwidth:30 nm; baseline method)
Dimensions
13.5 in (W) x 15.75 in (D) x12.0 in (D)
(340 mm (W) x 400 mm (D) x 300 mm (D))
Weight approx.
42 lbs (19 kg)
L-2400 UV/L-2420 UV/VisDetectors Specifications
Optics
Double beam and ratio mode
Calibration
Built-in Hg lamp
Range
L-2400: 190 to 600 nm
L-2420: 190 to 900 nm
Light source
L-2400: D2 lamp
L-2420: D2 lamp and W lamp
Accuracy
+/- 1 nm
Bandwidth
6 nm
Noise
< 0.6 x 10-5 AU
Drift
< 1.0 x 10-4 AU/h
AUFS range
0.25, 0.5, 1, 2 AU
Response
0.05, 0.1, 0.5, 1, 2, 4, 8 s
Programs
9 programmable steps
Max. Time
600 min
Max. Steps
100 (in 9 programs)
Available functions
Wavelength, time, autozero, and hold
GLP functions
Auto calibration using Hg lamp Lamp energy check
Log for usage
Replacement date
Serial number registration in unit memory
Safety
Bult-in leak sensor, Error handling
Dimensions
13.5 in (W) x 15.75 in (D) x 6.0 in (D)
(340 mm (W) x 400 mm (D) x 150mm (D))
Weight approx.
24 lbs (11 kg)
L-2455 Diode Array Detector Specifications
Optics

Single-beam photometric detector with grating monochromator and 1024-bit diode array
Light source
D2 and W lamps
Hg lamp for wavelength calibration
Wavelength range

190 - 900 nm
Noise
< 0.5 x 10-5 AU (at 250 nm and 600 nm)
Drift
< 0.5 x 10-3 AU/h (at 250 nm and 600 nm)
Slit width
1 nm or 4 nm
Wavelength time program
by EZChrom Elite
Spectrum scan function with background subtraction
by EZChrom Elite
GLP functions
Auto calibration using Hg lamp
Lamp energy check
Log for usage
Lamp replacement date
Serial number registration in unit memory
Safety
Leak sensor, Error handling
Input/Output contact signals
START IN
BUSY OUT
ERROR IN/OUT
Power requirements
24 V DC, 100 W
Dimensions
13.5 in (W) x 15.75 in (D) x 6.0 in (D)
(340 mm (W) x 400 mm (D) x 150mm (D))
Weight approx.
26 lbs (12 kg)
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Specifications
Agilent 6890
Agilent 6890N

Height

50 cm (19.7 in.)

50 cm (19.7 in.)

Width

58 cm (26.8 in.)

58 cm (26.8 in.)

Depth

54 cm (21.6 in.)

54 cm (21.6 in.)

Average Weight

49 kg (108 lb)

49 kg (108 lb)

Networkable

No

Yes

6890 Environmental Conditions

Ambient Operating
Temperature

15 ˚C to 35 ˚C

15 ˚C to 35 ˚C

Ambient Operating
Humidity

5-95 %

5-95 %

Storage Extremes

-40˚C to 65˚

-40˚C to 65˚

Line Voltage Requirements

±5% of nominal

±5% of nominal

Agilent 5890 Column Oven

Dimensions

28 x 31 x 16 cm

28 x 31 x 16 cm

Operating temperature

4˚C above ambient to 450˚C

4˚C above ambient to 450˚C

Maximum run time

120˚C/min

120˚C/min

Available Detectors for the
Agilent 6890 GC

Flame ionization detector (FID)
Thermal conductivity detector (TCD)
Micro-electron capture detector (micro-ECD)
Nitrogen-phosphorus detector (NPD)
Single- or dual-wavelength flame photometric detectors (FPD)
Atomic emission detector (AED)
Mass selective detector (MSD)

Flame ionization detector (FID)
Thermal conductivity detector (TCD)
Micro-electron capture detector (micro-ECD)
Nitrogen-phosphorus detector (NPD)
Single- or dual-wavelength flame photometric detectors (FPD)
Atomic emission detector (AED)
Mass selective detector (MSD)

FID

  • Maximum temperature: 450 oC
  • Detectivity: 2 pg C/sec
  • Linear dynamic range: 107
  • Patented ceramic flame tip: standard
  • Flame-out detection/auto re-ignition: standard

CP-1177 Split/Splitless

  • Pressure range: 0-100 psi
  • Total flow: 500 mL/min at 10 psi
  • Maximum temperature: 450 oC
  • Split range: 1-10,000 (column dependent)

Column Oven

  • Dimensions: 28 cm (w) x 20 cm (d) x 28 cm (h)
  • Temperature range: ambient +4 oC to 450 oC
  • With liquid N2: -99 oC to 450 oC
  • With liquid CO2: -65 oC to 450 oC
  • Temperature program ramps/holds: 7/8
  • Maximum temperature ramp rate: 100 oC /min for all voltages
  • Cool down rate: 400 oC to 50 oC in 4.5 minutes
  • Temperature set-point resolution: 1 oC

Dimensions and Weights

  • Size: 53 cm (h) x 66 cm (w) x 56 cm (d)
  • Weight: 43 kg
    • Empty tab. Edit page to add content here.
    Specifications
    Agilent 6890
    Agilent 6890N

    Height

    50 cm (19.7 in.)

    50 cm (19.7 in.)

    Width

    58 cm (26.8 in.)

    58 cm (26.8 in.)

    Depth

    54 cm (21.6 in.)

    54 cm (21.6 in.)

    Average Weight

    49 kg (108 lb)

    49 kg (108 lb)

    Networkable

    No

    Yes

    6890 Environmental Conditions

    Ambient Operating
    Temperature

    15 ˚C to 35 ˚C

    15 ˚C to 35 ˚C

    Ambient Operating
    Humidity

    5-95 %

    5-95 %

    Storage Extremes

    -40˚C to 65˚

    -40˚C to 65˚

    Line Voltage Requirements

    ±5% of nominal

    ±5% of nominal

    Agilent 5890 Column Oven

    Dimensions

    28 x 31 x 16 cm

    28 x 31 x 16 cm

    Operating temperature

    4˚C above ambient to 450˚C

    4˚C above ambient to 450˚C

    Maximum run time

    120˚C/min

    120˚C/min

    Available Detectors for the
    Agilent 6890 GC

    Flame ionization detector (FID)
    Thermal conductivity detector (TCD)
    Micro-electron capture detector (micro-ECD)
    Nitrogen-phosphorus detector (NPD)
    Single- or dual-wavelength flame photometric detectors (FPD)
    Atomic emission detector (AED)
    Mass selective detector (MSD)

    Flame ionization detector (FID)
    Thermal conductivity detector (TCD)
    Micro-electron capture detector (micro-ECD)
    Nitrogen-phosphorus detector (NPD)
    Single- or dual-wavelength flame photometric detectors (FPD)
    Atomic emission detector (AED)
    Mass selective detector (MSD)

    FID

    • Maximum temperature: 450 oC
    • Detectivity: 2 pg C/sec
    • Linear dynamic range: 107
    • Patented ceramic flame tip: standard
    • Flame-out detection/auto re-ignition: standard

    CP-1177 Split/Splitless

    • Pressure range: 0-100 psi
    • Total flow: 500 mL/min at 10 psi
    • Maximum temperature: 450 oC
    • Split range: 1-10,000 (column dependent)

    Column Oven

    • Dimensions: 28 cm (w) x 20 cm (d) x 28 cm (h)
    • Temperature range: ambient +4 oC to 450 oC
    • With liquid N2: -99 oC to 450 oC
    • With liquid CO2: -65 oC to 450 oC
    • Temperature program ramps/holds: 7/8
    • Maximum temperature ramp rate: 100 oC /min for all voltages
    • Cool down rate: 400 oC to 50 oC in 4.5 minutes
    • Temperature set-point resolution: 1 oC

    Dimensions and Weights

  • Size: 53 cm (h) x 66 cm (w) x 56 cm (d)
  • Weight: 43 kg